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Beilstein J. Org. Chem. 2020, 16, 3093–3103, doi:10.3762/bjoc.16.259
Graphical Abstract
Scheme 1: Benzylic addition of aldehydes to azaarenes using different catalysts.
Scheme 2: Synthesis of azaarene derivatives from different precursors.
Scheme 3: Our work: catalyst- and solvent-free benzylic addition of aldehydes to azaarenes.
Scheme 4: Large-scale experiments for the synthesis of 2-(6-methylpyridin-2-yl)-1-(4-nitrophenyl)ethan-1-ol (...
Scheme 5: Plausible mechanism for the formation of 2-(6-methylpyridin-2-yl)-1-(4-nitrophenyl)ethan-1-ol (3a) ...